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Course syllabus N418L10_4B - Laboratory of Instrumental Methods in Analysis (FCFT - WS 2017/2018)

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University: Slovak University of Technology in Bratislava
Course unit title:
Laboratory of Instrumental Methods in Analysis
Course unit code: N418L10_4B
Mode of completion and Number of ECTS credits:
Classified fulfillment of requirements (3 credits)
Name of lecturer:
Ing. Anna Lomenova, PhD. (examiner, instructor)
Ing. Alena Manová, PhD. (examiner, instructor, lecturer, person responsible for course) - slovak, english
Ing. Martin Němeček, PhD. (examiner, instructor)
Ing. Kristína Poláčeková Cinková, PhD. (examiner, instructor)
Ing. Jozef Sochr, PhD. (examiner, instructor)
Ing. Silvia Zichová, PhD. (examiner, instructor)
Learning outcomes of the course unit:
Provide advanced work using laboratory analytical techniques, basics of proper implementation of the analytical operations, good laboratory practice. Know the principles of creation of analytic signal measuring instruments and principles of optimization of various modes of measurement. Control instrumental analytical procedures for obtaining information and procedures evaluation of measurement results.
Prerequisites and co-requisites:
Course contents:
1.Basic principles work in the analytical laboratory . Working with measures of weight and
volume. Preparation of solutions. Titration technique.
2.Optical methods - the absorption methods of determination by the addition of standard and
nephelometric / turbidimetric methods of determination by the calibration line, the emission
spectrum methods. Identification of organic substances on the basis of a comprehensive
interpretation of spectra NMR, MS,IR.
3.Electroanalytical methods - voltammetry as analytical technique, study electrochemical
processes and potentiometric titration of acid mixtures. Derivative and Granov transform of
the titration curves. Polarography and biampermetrická titration, precise preparation of
the buffer solutions and pH measurement.
4.Chromatography techniques - liquid chromatography and gas chromatography in
quantitative analysis, the internal standard method and preconcentrate treatment techniques
of the samples, SPE. Liquid and gas chromatography as an identification method.
Recommended or required reading:
PURDEŠOVÁ, A. -- TARAPČÍK, P. -- SÁDECKÁ, J. -- HROBOŇOVÁ, K. -- ŠPÁNIK, I. -- RIEVAJ, M. -- ŠVORC, Ľ. -- MANOVÁ, A. -- ČACHO, F. Praktikum z analytickej chémie. Bratislava : Nakladateľstvo STU, 2011. 242 p. ISBN 978-80-227-3555-1.
BUSTIN, D. -- HLADKY, Z. -- GARAJ, J. Analytická chémia. Alfa, Bratislava: SNTL, Praha, 1987. 744 p.

Planned learning activities and teaching methods:
Subject is realized through laboratory exercises.
Assesment methods and criteria: There will be one written clearance for 20 points during the semester.
For an evaluation "A" must be obtained at least 90 points of a total 100 points,
"B" at least 80 points,
"C" at least 70 points,
"D" at least 60 points,
"E" at least 50 points.
Credits shall not be granted to a student who obtains a written clearance less than 10 points.
Language of instruction: Slovak, English
Work placement(s): There is no compulsory work placement in the course unit.

Last modification made by Ing. Tomáš Molnár on 09/22/2017.

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