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Course syllabus N418L10_4B - Laboratory of Instrumental Methods in Analysis (FCFT - WS 2017/2018)

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University: Slovak University of Technology in Bratislava
Faculty: Faculty of Chemical and Food Technology
Course unit code: N418L10_4B
Course unit title: Laboratory of Instrumental Methods in Analysis
Mode of delivery, planned learning activities and teaching methods:
laboratory/construction practice3 hours weekly (on-site method)

Credits allocated: 3
Recommended semester/trimester: Automation, Information Engineering and Management in Chemistry and Food Industry - bachelor (compulsory), 5. semester
Automation, Information Engineering and Management in Chemistry and Food Industry - bachelor (compulsory), 5. semester
Biotechnology - bachelor (compulsory), 5. semester
Food, Nutrition, Cosmetics - bachelor (compulsory), 5. semester
Chemical Engineering - bachelor (compulsory), 5. semester
Level of study: 1.
Prerequisites for registration: none
Assesment methods:
Practical execution of all laboratory exercises and test.
Learning outcomes of the course unit:
Provide advanced work using laboratory analytical techniques, basics of proper implementation of the analytical operations, good laboratory practice. Know the principles of creation of analytic signal measuring instruments and principles of optimization of various modes of measurement. Control instrumental analytical procedures for obtaining information and procedures evaluation of measurement results.
Course contents:
1.Basic principles work in the analytical laboratory . Working with measures of weight and
volume. Preparation of solutions. Titration technique.
2.Optical methods - the absorption methods of determination by the addition of standard and
nephelometric / turbidimetric methods of determination by the calibration line, the emission
spectrum methods. Identification of organic substances on the basis of a comprehensive
interpretation of spectra NMR, MS,IR.
3.Electroanalytical methods - voltammetry as analytical technique, study electrochemical
processes and potentiometric titration of acid mixtures. Derivative and Granov transform of
the titration curves. Polarography and biampermetrická titration, precise preparation of
the buffer solutions and pH measurement.
4.Chromatography techniques - liquid chromatography and gas chromatography in
quantitative analysis, the internal standard method and preconcentrate treatment techniques
of the samples, SPE. Liquid and gas chromatography as an identification method.
Recommended or required reading:
PURDEŠOVÁ, A. -- TARAPČÍK, P. -- SÁDECKÁ, J. -- HROBOŇOVÁ, K. -- ŠPÁNIK, I. -- RIEVAJ, M. -- ŠVORC, Ľ. -- MANOVÁ, A. -- ČACHO, F. Praktikum z analytickej chémie. Bratislava : Nakladateľstvo STU, 2011. 242 p. ISBN 978-80-227-3555-1.
BUSTIN, D. -- HLADKY, Z. -- GARAJ, J. Analytická chémia. Alfa, Bratislava: SNTL, Praha, 1987. 744 p.

Language of instruction: slovak or english
Courses evaluation:
Assessed students in total: 360

31,7 %35,0 %26,4 %6,4 %0,5 %0 %
Name of lecturer(s): Ing. Anna Lomenova (examiner, instructor)
Ing. Alena Manová, PhD. (examiner, instructor, lecturer, person responsible for course) - slovak, english
Ing. Martin Němeček (examiner, instructor)
Ing. Kristína Poláčeková Cinková, PhD. (examiner, instructor)
Ing. Jozef Sochr, PhD. (examiner, instructor)
Ing. Silvia Zichová (examiner, instructor)
Last modification: 22. 9. 2017
Supervisor: Ing. Alena Manová, PhD. and programme supervisor

Last modification made by Ing. Tomáš Molnár on 09/22/2017.

Type of output: