Oct 16, 2019   10:49 p.m. Vladimíra
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Course syllabus N418V0_4I - Analytical Measurement Data Evaluation (FCFT - SS 2018/2019)


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University: Slovak University of Technology in Bratislava
Faculty: Faculty of Chemical and Food Technology
Course unit code: N418V0_4I
Course unit title: Analytical Measurement Data Evaluation
Mode of delivery, planned learning activities and teaching methods:
seminar2 hours weekly (on-site method)

 
Credits allocated: 2
 
Recommended semester/trimester: Biotechnology - master (optional), 2. semester
Biotechnology - master (optional), 2. semester
Level of study: 2.
Prerequisites for registration: none
 
Assesment methods:
written test
 
Learning outcomes of the course unit:
Students will take practice and will be in detail familiar in methods of interpretation and evaluation of chemical analysis data. Absolvent can evaluate uncertainties of measurement results.
 
Course contents:
Calculation techniques for approximate data, principles of handling with approximate numbers.
Rounding and correct record of results of calculation results.
Laboratory diary records, correct chemical and analytical terms. Plots and correct construction of graphs.
Methods of description and calculation of mixture concentrations. Stoichiometry and laws of conservation (mass, charge)
Measurement of weight and volume in analytical chemistry. Solution preparation and uncertainty of concentration of prepared solution. Dilution and uncertainty of final concentration.
Calculation of simple direct volumetric determination and uncertainty of result. Back titration and uncertainty of its result.
Gravimetric determination and its result uncertainty.
Effect of condition at chemical analysis on determination result, trueness. Indication of chemical reaction stoichiometry, condition for completeness of reaction, completeness of separation, precipitation, impact of interferences.
Application of basic statistic procedures in evaluation of analytical data. error, deviation and uncertainty. Averages, median, result as interval, basic distribution of stochastic quantities. Outliers. Basic statistical tests.
Calibration and standardization. corrections. Regression. Calculation of determination result from linear calibration line. Nonlinear calibration curve. Uncertainty of results obtained from calibration curve. Calibration by standard addition method, application, uncertainty of result.
Impact of noise in instrumental procedures of analytical measurements.
 
Recommended or required reading:
Basic:
GARAJ, J. -- LABUDA, J. Analytická chémia I. Bratislava: Vydavateľstvo STU, 1996. 188 p. ISBN 80-227-0838-0.
TARAPČÍK, P A K. Analytická chémia I. Zbierka príkladov. Bratislava : SVŠT v Bratislave, 1990. 105 p.
TARAPČÍK, P A K. Analytická chémia: Seminárne cvičenia - riešené príklady. Bratislava : STU v Bratislave, 2001. 145 p. ISBN 80-227-1469-0.
BUSTIN, D. Analytická chémia II. Bratislava: STU v Bratislave, 1996. 213 p. ISBN 80-227-0885-2.
LABUDA, J. -- TARAPČÍK, P. -- GARAJ, J. -- HROUZKOVÁ, S. -- LEHOTAY, J. -- MANOVÁ, A. -- SÁDECKÁ, J. Príručka vybraných pojmov v analytickej chémii. Bratislava : Nakladateľstvo STU, 2012. 205 p. ISBN 978-80-227-3769-2.
PURDEŠOVÁ, A. -- TARAPČÍK, P. -- SÁDECKÁ, J. -- HROBOŇOVÁ, K. -- ŠPÁNIK, I. -- RIEVAJ, M. -- ŠVORC, Ľ. -- MANOVÁ, A. -- ČACHO, F. Praktikum z analytickej chémie. Bratislava : Nakladateľstvo STU, 2011. 242 p. ISBN 978-80-227-3555-1.

 
Language of instruction: slovak or english
 
Notes:
 
Courses evaluation:
Assessed students in total: 5

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Name of lecturer(s): prof. Ing. Ján Labuda, DrSc. (person responsible for course) - slovak, english
Ing. Pavel Májek, PhD. (examiner, instructor, lecturer) - slovak, english
 
Last modification: 19. 2. 2018
Supervisor: prof. Ing. Ján Labuda, DrSc. and programme supervisor


Last modification made by Ing. Tomáš Molnár on 02/19/2018.

Type of output: