Sep 20, 2019   11:40 a.m. Ľuboslav, Ľuboslava
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Course syllabus N418C0_4B - Chemical Processes in Analytical Measurements (FCFT - WS 2019/2020)


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University: Slovak University of Technology in Bratislava
Faculty: Faculty of Chemical and Food Technology
Course unit code: N418C0_4B
Course unit title: Chemical Processes in Analytical Measurements
Mode of delivery, planned learning activities and teaching methods:
lecture2 hours weekly (on-site method)

 
Credits allocated: 2
 
Recommended semester/trimester: Biotechnology - bachelor (optional), 3. semester
Food, Nutrition, Cosmetics - bachelor (optional), 3. semester
Level of study: 1.
Prerequisites for registration: none
 
Assesment methods:
Test
 
Learning outcomes of the course unit:
Student will receive information about analytical signal generation based on chemical reactions, knowledge about sampling principles and sample treatment by chemical procedures; principles and application chemical methods of analysis, chemical aspects of instrumental analytical methods.
 
Course contents:
Process of chemical analysis and its selectivity, preparation and execution of measurement, reference materials.
Sampling, sample treatment and sample storage. Sample decompositions, preseparation and preconcentration, special techniques.
Preliminary tests in organic compound analysis.
General principles of analytical methods based chemical reactions. Acid–base reactions, redox reactions, complex and precipitation reactions. Qualitative analysis, selectivity and interferences.
Quantitative analysis based on chemical reactions. Procedures of volumetric analysis, titration curve, indication. Chemical aspects in volumetric analysis. Gravimetry and precipitation from solution; condition and application.
Chemical reactions in organic compound analysis: methods of elemental analysis, functionals groups detection and determination.
Rate of chemical reaction as source of analytical signal.
Chemical modification of analyte. Extraction techniques in sample treatment. Solid phase extraction (SPE, SPME, SBSE). Ion exchange in selective separation and concentration of analytes. Recovery.
Chemical aspects in instrumental analytical procedures. Reactions in coulometry, voltamperometry. Separation principles in dynamic methods (chromatography and electromigration). Derivatization in chromatography.
 
Recommended or required reading:
Basic:
GARAJ, J. -- LABUDA, J. Analytická chémia I. Bratislava: Vydavateľstvo STU, 1996. 188 p. ISBN 80-227-0838-0.
PURDEŠOVÁ, A. -- TARAPČÍK, P. -- SÁDECKÁ, J. -- HROBOŇOVÁ, K. -- ŠPÁNIK, I. -- RIEVAJ, M. -- ŠVORC, Ľ. -- MANOVÁ, A. -- ČACHO, F. Praktikum z analytickej chémie. Bratislava : Nakladateľstvo STU, 2011. 242 p. ISBN 978-80-227-3555-1.
BUSTIN, D. Analytická chémia II. Bratislava: STU v Bratislave, 1996. 213 p. ISBN 80-227-0885-2.
LABUDA, J. -- TARAPČÍK, P. -- GARAJ, J. -- HROUZKOVÁ, S. -- LEHOTAY, J. -- MANOVÁ, A. -- SÁDECKÁ, J. Príručka vybraných pojmov v analytickej chémii. Bratislava : Nakladateľstvo STU, 2012. 205 p. ISBN 978-80-227-3769-2.

 
Language of instruction: slovak or english
 
Notes:
 
Courses evaluation:
Assessed students in total: 7

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Name of lecturer(s): doc. Ing. Ľubomír Švorc, PhD. (person responsible for course)
 
Last modification: 16. 7. 2019
Supervisor: doc. Ing. Ľubomír Švorc, PhD. and programme supervisor


Last modification made by Ing. Tomáš Molnár on 07/16/2019.

Type of output: