Dec 7, 2019   0:05 a.m. Ambróz
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Course syllabus N419L2_4I - Laboratory of Spectral Methods (FCFT - WS 2019/2020)


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University: Slovak University of Technology in Bratislava
Faculty: Faculty of Chemical and Food Technology
Course unit code: N419L2_4I
Course unit title: Laboratory of Spectral Methods
Mode of delivery, planned learning activities and teaching methods:
laboratory/construction practice5 hours weekly (on-site method)

 
Credits allocated: 5
 
Recommended semester/trimester: Technical Chemistry - master (semi-compulsory), 3. semester
Level of study: 2.
Prerequisites for registration: none
 
Assesment methods:
Elaboration of two projects on the use of spectral methods for the characterization of inorganic compounds and their successful presentation.
 
Learning outcomes of the course unit:
In laboratory tutorials the student will learn:

a) Measurement of IR spectra of complex compounds by KBr, Nujol and ATR technique.

b)Measurement of Raman spectra of complex compounds.

c)Measurement of electron spectra of complex compounds by Nujol technique as well as in solutions of organic solvents.

d)Measuring the EPR spectra of Cu (II) complexes.
 
Course contents:
1. Infrared spectroscopy of coordination compounds. The experimental technique. Methods of measurement and treatment of samples.

2. Raman spectroscopy of coordination compounds. The experimental technique. Methods of measurement and treatment of samples.

3. Molecular spectroscopy in the ultraviolet and visible region. The experimental technique. Methods of measurement and treatment of samples.

4. EPR spectroscopy of inorganic and coordination compounds.

5. The use of tutorials to determine the structure of unknown compounds.
 
Recommended or required reading:
Basic:
MILATA, V. -- BREZOVÁ, V. -- SEGĽA, P. Aplikovaná molekulová spektroskopia. Bratislava: STU, 2008. 602 p. ISBN 978-80-227-2960-4.
MILATA, V. -- SEGĽA, P. Spektrálne metódy v chémii + CD-ROM. Bratislava : Vydavateľstvo STU v Bratislave, 2004. 327 p. ISBN 80-227-2049-6.

 
Language of instruction: slovak or english
 
Notes:
 
Courses evaluation:
Assessed students in total: 20

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Name of lecturer(s): prof. RNDr. Milan Mazúr, DrSc. (instructor) - slovak, english
prof. Ing. Peter Segľa, DrSc. (examiner, instructor) - slovak, english
Ing. Jozef Švorec, PhD. (examiner, instructor, person responsible for course) - slovak, english
 
Last modification: 29. 1. 2019
Supervisor: Ing. Jozef Švorec, PhD. and programme supervisor


Last modification made by Ing. Tomáš Molnár on 01/29/2019.

Type of output: