Sep 16, 2019   11:05 a.m. Ľudomila, Ľudmila
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Course syllabus N418A7_4I - Analytical Separation Methods II (FCFT - SS 2019/2020)


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University: Slovak University of Technology in Bratislava
Faculty: Faculty of Chemical and Food Technology
Course unit code: N418A7_4I
Course unit title: Analytical Separation Methods II
Mode of delivery, planned learning activities and teaching methods:
lecture2 hours weekly (on-site method)
seminar1 hour weekly (on-site method)

 
Credits allocated: 4
 
Recommended semester/trimester: Technical Chemistry - master (semi-compulsory), 2. semester
Technical Chemistry - master (semi-compulsory), 2. semester
Level of study: 2.
Prerequisites for registration: none
 
Assesment methods:
credits, individual written and oral exam
 
Learning outcomes of the course unit:
Students know fundamentals of the theoretical basis of the liquid chromatography methods and electromigration separation methods. They are able to apply them to the analysis of multicomponent samples and for determination of trace concentrations of organic compounds from technological and natural materials.
 
Course contents:
Theoretical basis of separation by high performance liquid chromatography
Properties and selection of stationary and mobile phases
The mechanism of separation for the different chromatographic systems
Instrumentation in liquid chromatography
Detection in liquid chromatography
A direct connection of column liquid chromatography with spectral methods
Derivatization of the analytes
Enantioselective separation
Theoretical basis of separation by electromigration separation methods
The electrophoretic migration and electroosmotic flow
Instrumentation for capillary electrophoresis
Capillary zone electrophoresis and capillary gel electrophoresis
Capillary isotachophoresis and capillary isoelectric focusing
Analytical applications
 
Recommended or required reading:
Basic:
LEHOTAY, J. Separačné metódy v analytickej chémii. Bratislava: STU v Bratislave, 2009. 235 p. ISBN 978-80-227-3036-5.
Encyclopedia of chromatography. In.
CAZES, J. Encyclopedia of chromatography: 3 Vol. Boca Raton : CRC Press, 2010. ISBN 978-1-4200-8459-7.
POOLE, C F. The Essence of Chromatography. Amsterdam : Elsevier, 2003. 925 p. ISBN 0-444-50199-1.

 
Language of instruction: -- item not defined --
 
Notes:
 
Courses evaluation:
Assessed students in total: 89

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22,5 %42,7 %30,3 %4,5 %0 %0 %
Name of lecturer(s): doc. Ing. Katarína Hroboňová, PhD. (person responsible for course) - slovak
 
Last modification: 29. 1. 2019
Supervisor: doc. Ing. Katarína Hroboňová, PhD. and programme supervisor


Last modification made by Ing. Tomáš Molnár on 01/29/2019.

Type of output: