19. 10. 2019  16:26 Kristián
Akademický informační systém

Sylabus předmětu N400P0_4D - Advanced Separation Methods (FCFT - 2019/2020 - post-graduate studies)


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University: Slovak University of Technology in Bratislava
Faculty: Faculty of Chemical and Food Technology
Course unit code: N400P0_4D
Course unit title: Advanced Separation Methods
Mode of delivery, planned learning activities and teaching methods:
lecture2 hours weekly (on-site method)

 
Credits allocated: 3
 
Recommended semester/trimester: Analytical Chemistry - doctoral (optional), 1. year
Analytical Chemistry - doctoral (optional), 1. year
Level of study: 3.
Prerequisites for registration: none
 
Assesment methods:
individual written and oral exam
 
Learning outcomes of the course unit:
Students know fundamentals of concepts and terminology of advanced separation and identification methods, advanced chromatographic methods and combined techniques, ambient mass spectrometry techniques. Students learn modern identification methods.
 
Course contents:
Treatment of the sample before analysis
Fast separation and automated systems
Detection in chromatographic techniques
Possibilities of derivatisation and its use
Separation in trace and ultra-trace analysis
Mass spectrometry
Identification of compounds by mass spectra
Interpretation of MS spectra, MS quantification
Identification of compounds by NMR
Possibilities of interferences during identification and determination
Combination of spectroscopic methods for the structure analysis of organic compounds
 
Recommended or required reading:
Basic:
POOLE, C F. The essence of chromatography. Amsterdam: Elsevier, 2003. 925 p. ISBN 0-444-50199-1.
OTTO, M. -- MERMET, J M. -- KELLNER, R. Analytical Chemistry, A Modern Approach to Analytical Science. Weinheim: Wiley-VCH, 2004. 1181 p. ISBN 978-3-527-30590-2.
LEHOTAY, J. Separačné metódy v analytickej chémii. Bratislava: STU v Bratislave, 2009. 235 p. ISBN 978-80-227-3036-5.
LABUDA, J. -- TARAPČÍK, P. -- GARAJ, J. -- HROUZKOVÁ, S. -- LEHOTAY, J. -- MANOVÁ, A. -- SÁDECKÁ, J. Príručka vybraných pojmov v analytickej chémii. Bratislava : Nakladateľstvo STU, 2012. 205 p. ISBN 978-80-227-3769-2.

 
Language of instruction: slovak and english
 
Notes:
 
Courses evaluation:
Assessed students in total: 12

PN
100,0 %0 %
Name of lecturer(s): doc. Ing. Katarína Hroboňová, PhD. (person responsible for course) - slovak, english
 
Last modification: 26. 4. 2019
Supervisor: doc. Ing. Katarína Hroboňová, PhD. and programme supervisor


Last modification made by Ing. Tomáš Molnár on 04/26/2019.

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